MSY-7100 High-Temperature Magnetic Field Heating (Annealing) Furnace|SeeweTek | Magnetic Field Generators, Magnetic Testing Solutions, Physical Property Testing Solutions

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MSY-7100 High-Temperature Magnetic Field Heating (Annealing) Furnace
Description:The high-temperature magnetic field heating furnace can simultaneously subject the sample to a strong magnetic field, high vacuum, and high temperature. It can also use any combination of these three experimental environments to meet the testing requirements of different samples under various conditions. Scope of application: Various soft magnetic materials that require heating or demagnetization in high-temperature, high-vacuum, and strong magnetic field environments.
Detail
Parameter
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Equipment Principle

The high-temperature vacuum magnetic field heating furnace system produced by our company consists of a heating furnace, heating furnace power supply, Labview control software (optional), electromagnet, high-precision bipolar constant current power supply, molecular pump set, and water cooling unit, forming a feedback-regulated heating system.

In this system, the mechanical pump (dry pump optional) in the molecular pump set first roughs the vacuum chamber (sample chamber). When the ultimate vacuum for starting the molecular pump is reached, the molecular pump is started for high-vacuum pumping to achieve the required vacuum level. By opening the software and inputting the desired magnetic field and temperature values, the temperature of the sample inside the equipment is automatically controlled and stabilized at a certain value through closed-loop feedback regulation. The software can complete the experiment according to the experimental conditions set by the user.

  • Magnetic field control: Users can directly set the required magnetic field size through the software. The actual magnetic field value is read by a high-precision gaussmeter and fed back to the high-precision constant current power supply. After processing by the internal software of the power supply, the output current of the high-precision constant current power supply is directly controlled to achieve the desired magnetic field, which is displayed in real time on the software.
  • Temperature control: By directly setting the required temperature value on the human-machine interface of the software, the computer software processes the command and sends it to the heating furnace temperature controller. The controller reads the actual temperature of the sample area through a temperature sensor (thermocouple) and adjusts the output current using its internal fuzzy control PID regulation to stabilize the temperature within a certain accuracy range, thus achieving the different temperatures required by the user.
  • Vacuum environment: The vacuum environment is obtained through the molecular pump set, displayed and monitored by a high-vacuum full-range vacuum gauge, and the detection results are transmitted to the computer in real time.
  • Annealing process: The sample is heated in a strong magnetic field (or non-magnetic) environment to a certain temperature (set by the user) and maintained at that temperature. Then a magnetic field is continuously applied (which can be changed at any time). After achieving the user's purpose, the magnetic field and heating environment are turned off, and the sample is cooled to room temperature.

System Block Diagram


  • The vacuum chamber and main components are made of high-quality non-magnetic 304 stainless steel.
  • The vacuum system uses a molecular pump set; vacuum measurement uses a digital full-range vacuum gauge.
  • Vacuum degree and leak rate: ① Ultimate vacuum of vacuum chamber: 6×10-4 Pa (cold state); ② Leak rate: <10-11 Pa·L/s. Vacuum degree may fluctuate with temperature changes, which is normal.
  • From room temperature to 900°C, heating rate better than 100 K/min, temperature control accuracy: ±1°C.
  • During heating, the heating wire is encapsulated in a quartz tube, greatly reducing contamination of the sample surface due to volatilization of the heating wire.
  • Customizable electromagnet.
  • Magnetic field strength: Better than 2.5 T at 10 mm gap, better than 1.2 T at 50 mm gap.
  • Can operate continuously and stably for more than 24 hours.
  • Electromagnet pole gap continuously adjustable.
  • Coil cooling method: water cooling.
  • Matching magnet power supply: Bipolar constant current power supply, stability better than ±25 ppm/h, smooth zero crossing without dead spots.
  • Matching electromagnet: Long-term operation stability < ±0.5 Gs.
  • Supports magnetic field mode and current mode control output; with RS232 interface.
  • Built-in gaussmeter and probe in the power supply.
  • The built-in gaussmeter must be integrated with the power supply, allowing direct setting and achievement of the required magnetic field through the power supply panel, forming a closed-loop control of the magnetic field, thus enabling precise control of the actual magnetic field. An independent gaussmeter cannot be used.
  • Measurement range: 0-3 T.
  • Minimum resolution: 0.01 Gs.
  • Cooling method: air cooling.
  • High-temperature furnace and temperature controller.
  • Outer diameter of high-temperature furnace ≥ 50 mm.
  • Molecular pump pumping speed (for nitrogen) ≥ 600 L/s, inlet flange ≤ KF40.
  • Ultimate vacuum of molecular pump better than 6×10-6 Pa.
  • Integrated circulating water chiller, cooling capacity ≥ 8 kW @25°C, water tank volume ≥ 90 L, outlet water temperature 5-35°C, temperature control accuracy ±1°C.
Magnetic Field Configuration
Furnace ModelDimensionsSample Chamber SizeMax TemperatureElectromagnet Field
GC800-15Φ57×400mmφ15×150mm900°C1.15T@EM7 0.8T@EM5
GC800-30φ68×400mmφ30×150mm900°C1.0T@EM7 0.68T@EM5


System Configuration

  • Vacuum heating furnace and controller
  • Vacuum acquisition and measurement equipment
  • Strong magnetic field acquisition equipment (electromagnet)
  • Circulating water chiller equipment

Configuration List

No.ModelDescriptionQty
1MSY-7100Vacuum heating furnace1 set
2Sample cup for heating furnace (powder, film)1 set
3-401Heating controller1 set
4Furnace support bracket for positioning in electromagnet1 set
5EM7EM7 electromagnet power supply (25/190SA), built-in high-precision gaussmeter1 set
6F600Molecular pump set: 1) F600 molecular pump; 2) Dry mechanical pump; 3) Vacuum gauge, etc.1 set
7KD3ASWTCirculating water chiller 8KW1 set
8Control software (optional): Directly set magnetic field, temperature, timing, etc. via computer; data storage, printing, etc.1 set